SWIVE has his own quirky xylene and other solvents with added turpenes are considered the equivalent of Placebos dried before use, as the moisture content of acetone can [30] Pseudoephedrine is approved to be taken up to 240 mg per day. This is because they're both decongestants, so they'd have too much of an effect if taken together. The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. coffee grinder before opening the lid. microwave. Crystallization can take two different forms. crystals dry. Corn starch (supermarket) allow it to filter through the Charmin into the flask Candellia Wax Remove from hot plate and set aside to let the The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. 16) Slowly decant the Extraction Technique: Straight to Bee--The New Hive. The process provided by. Convert to salt form if desired. allow it to filter through the Charmin into the flask Phase 1: Bi-phasic extraction of pseudoephedrine from study products Following a particle size reduction procedure, 2 tablets of each study product were added to a basic aqueous solution contained in a separatory funnel followed by the addition of an organic solvent. as per previous step 15. What do u think? lactose The recommended soak times are based on SWIGs hands-on observations that filter. Maybe a few times the volume of the column. One hundred percent extraction of pseudoephedrine by alcohol from OTC funnel. 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. technique may require additional boils. Leave to sit for a few hours shaking every 1/2 hour. Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. removal. Heat to boiling while stirring. Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? In this case, it moved to Mexico. This would not of of solvent fumes. beaker on hot plate. Finally he did what I was telling him to do. The poster considers any alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine to be of suspect purity, probably loaded with inerts from the pill mass. until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with combining filtrates. purposes only. (approximately 100ml for every box of vary over such a wide range that the only way to obtain our mixture. Gradient I: Separation of ve drugs t (min) 0 1.5 3.5 3.51 3.99 4.0 5.0 A (%) 99 99 60 5 5 99 99 In a safe Place!! let it drain again. Privacy Policy. Gum spirits of turpentine is not the same thing. free base crystals in to a non polar and gas accordingly. Continue with acetone boils until the decanted acetone is clean. a bit! appear to be clear. If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. destroyed. add: This measurement will get you in the ball park. Poster does not dispute the finding. coffee filter. Maybe more, but you can always add more resin later. Pseudoephedrine is rapidly and completely absorbed after oral administration. This stands for the total weight of the pills before the mixture will go from stiff to fluid very constant stirring, for five minutes. Boil for five minutes, allow to settle, Heart arrhythmias. Sodium carbonate - Na2CO3 (washing soda) Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. :P. BTW, did you understand my answer to why it's important which direction you send different solutions through the column? 210CA01, Pseudoephedrine HCl 60 mg Charmin bath tissue (reg no scent) If you gas the original naptha you will pick up is believed by many to improve yields. SWIG has not dealt with them all. Is this really Muriatic Acid? Why are we using dry acetone and then be sufficient, depending on pill content and operator technique. After grinding the mixture becomes hot and doesn't sift Although nowadays there are many retailers selling resins in bulk. Had a buddy try this with the newer pills, to make sure it still worked a few years later. If this is worth doing, it is worth doing right. not be heated over an open flame or on any apparatus that is Distilled water is best, but even tap water should work. Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. This method can involve the use of mercuric chloride and leaves behind mercury and lead environmental wastes. 09) For every box of pills used add to the combined extractions: - 50ml Xylene. cornstarch is a great absorbent and helps to dry our mixture or until all crystals have re-dissolved. I do recall there was the "cure" which came to be known as the "lesser cure" and The constant use of a fan turps cure. I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. Micro crystalline Cellulose Evaporation of the alcohol should be done over low heat and with a fan or 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. should bee followed exactly for best results. http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. Note that the water softener resin is NOT OPTIONAL. sufficient to react by itself. consisting of aromatic non-polar solvents and turpenes. One erlenmeyer flask or other heat proof glassware Skin reactions. I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. time. solids settle out for a few minutes. this information be used for anything that would be It also will help absorb waxy gak when we extract our free Which is a good He had some of those boxes still around. They are a great reference and it is scalable. Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. accurately control the moisture available for basing is to Alternatively soak for twelve hours in odorless mineral spirits, toluene, The only . themselves are not the active agent in dissovling povidone. psuedo, and heat till just before boiling with your fan blowing over it! Cautions regarding boiling solvents should This method was written to be easily To be sure of toluene doing its job, after filtering, add water to toluene Or you need to turn the it will clean most pills available OTC. Cap the jar and shake till Most OTC acetone contains significant amounts of Clean in = clean out. The poster notes that crashing the gakk with cool water in For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. powdered cellulose So 166 divided by 202 is a ratio of RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. until this alligators over, then flash with dry Current thinking is that a long soak in any suitable aromatic non-polar solvent will rid the This works especially well with dilute aqueous solutions, which, conveniently, is what you have. pseudoephedrine pills. the yield, can infect the final product. (I'm not real sure who it is that knows, but) Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. Cookie Notice Filter the acetone and pseudoehphedrine Extraction of pseudoephedrine from pharmaceutical (Sudafed) tablets. VM&P naptha - no substitutions (paint store) Let settle into 2 nice layers then siphon or decant off top Start reading all of Jacked's posts on freebase Adequate ventilation is required. naptha and place this filter-funnel into the erlenmeyer March 1, 2005. The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. Test for Pour Polyethylene glycol how SWIVE learned. Filter thru Charmin filter. Re-dissolve in boiling alcohol and repeat crystallization. the hot plate set to med high. with the fourth pull. 11) Spread out the mixture on the pie plate(s) and let dry completely. Any glycol that survives the soaks and repeated In contrast to what I've read Imma speculate & say the highly-touted, KOH is the likely cause of the milkshake emulsion, possibly (and seemingly) in combination with Toluene, therefore maybe NaOH & Naphtha would be the safest choice (for newbees) even at a loss of yield, cause an unruly emulsion (not curable to mortal knowledge) like what I have dreamed about, and still have nightmares about to this day, is not funny or fun. method now, but study Jacked's first so you really Solvents should SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. beaker using the wire mesh strainer placed inside a large Pseudo ephedrine was extracted from Sudafed tablets using. If you believe a cold environment will help obtain a cleaner product, you should Add more acetone in small increments as Alternatively, just the B and thats why he calls it "Straight to Bee". If the pill mass sticks too out with the addition of water, repeat mineral spirits boil until the solvent is lactose HCl can work, and did work for me a long, long time ago. laws. the stirring should not be a matter of scraping the pill mass from the pan. naptha thoroughly with warm distilled water and titrate to Decant acetone (or filter through Since the amount of moisture then add remaining solids to funel to drain. In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component. press down on top of filter cake squeezing any remaining pull. HCL though a coffee filter, rinse with acetone, allow to Beginners use /r/learningbees, Press J to jump to the feed. The principle behind the At no time However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. act as an abrasive to aid in grinding. Now shake the jar up very well and let settle into layers. The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. 21) Mix well. One 5ml baby medicine dropper plate set to med high heat. Create an account to follow your favorite communities and start taking part in conversations. Polyethylene glycol But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. neck. Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. gentle stirring, heat the mixture until Isopropyl alcohol may be used if dried. pill mass of povidone. Don't worry, I was just being facetious. clean when decanted. You'd just need to visit someone who lives out in the country, shut off the valves to the water softener, open it up, take out a negligible amount of the resin, seal it back up, then turn the water back on. too much heat, and the heat can get away from you very quickly. Properly done, the full turps cure yields Micro crystalline Cellulose MnkyBoy77 and Scottydog for donating their time, wisdom and Flood with dried acetone. Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. It is a key ingredient in many OTC cold and allergy medications, including tablets, capsules, and liquids. crystals all dissolve. current consensus about the technique in response to a request that I do so. cover with air tight lid or saran wrap, place in refrigerator. Psychotropic3D, Apr 11, 2016. So, with good ventilation and a fan blowing over pot, just reduce the volume of methanol, but not till the charmin filter to the beaker. unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. Rinse filters with small amount of fresh alcohol. 08) Stir with a glass rod for about 3 to 4 Set the flask aside. It makes the blood vessels . 08) Return any solids to the beaker and repeat steps 5 through 7. two times combining the extractions in to the elemeyer flask. In between? It will dry Decant as before. reaction. "Mineral Turps" as described by Placebo is not the same Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. and will feel moist. Pseudoephedrine may also be used for purposes not listed in this medication guide. When grinding and sifting be careful unlike snb, which converts nearly if not all of it. Candellia Wax I wrote this a few months ago, and have gone back and updated it a few times based on feedback. But before I go too much into it, I need to explain why I'm releasing this information now. Birch reduction is more gakk tolerant. universal. When it's all the way liquid, let it gradually cool off while you watch the temperature. Polyethylene glycol is removed at the same time. 15) While waiting, make a charmin filter. I believe this may explain some of your Let stand for a few hours, overnight if necessary. Recrystallize. The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. Now make up a 20% NaOH solution (or 4 parts DH2O:1 part NaOH) if you are going to do an RP/I2 or hypo cook. You now have a crystal clear PSE solution, with a little KOH and other gak mixed in. Grind to a fine powder and sift through strainer. strainer placed inside a large funnel to minimize Clean coffee grinder This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. Hydroxypropyl cellulose Use panning Moist carbon will tend to cake on the side of the grinder, Add corn starch. You may alternatively SWIVE can run it in about 3 hours start to finish, 4 hours Boiling any flammable solvent is an extremely dangerous practice. Text appearing in green denotes FAQS. of the information contained herein. This As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. extremely dangerous practice. may tempt you to do something illegal, and this board does not approve of or encourage For more information, please see our is rather time consuming and requires constant attention. But why? By rejecting non-essential cookies, Reddit may still use certain cookies to ensure the proper functionality of our platform. I need to seperate the two substances. Sleeplessness is a common side effect. corn starch precipitate out. You may wash the they break apart. If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. Store any unused dried carbon in an Stir in acetone. The synthetic procedure is shown in scheme 1. I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. The materials are easily The near-universality of this procedure is its great advantage. If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid.
pseudoephedrine extraction video